ANALYTICAL SOLUTIONS GCANALYTICAL SOLUTIONS

GC
ANALYTICAL
SOLUTIONS
ENV 47
ENVIRONMENTAL
Sample Description:
8081 Organochlorine Pesticides on BPX50
8081 mix with internal standards 10mg/L, 5ng per component on column
BPX50 column
Phase:
Column:
BPX50, 0.25µm film
30m x 0.25mm ID
Column Part No. 054751
12
15
20
17
7
5
1
2
0
5
3 4
8 9 10
11
6
10
21
13 14
18
16
19
22
15
20
minutes
15
12
18
20
21
14
8
13
10
9
17
16
11
minutes
15
16
Sample Introduction:
Split / Splitless
Injector Temp:
240¡C
Injection Volume:
1µL
Autosampler Syringe: 5µL Fixed Needle
Part No. 001810
Septa:
Auto-Sep Tª
Part No. 041882
Injection Type:
Purge On Time:
Purge On (Spilt) Vent:
Split Ratio:
Liner Type:
19
Splitless
0.5min
60mL/min
NA
Single taper
Part No. 092017
minutes
17
Pressure/Flow Values:
Carrier Gas:
Helium
Constant Flow:
On
Pressure:
14.1psi
Column Flow:
1.3mL/min
Linear Velocity:
30cm/sec @ 40¡C
Oven Parameters:
Initial Temp:
Initial Time:
Rate 1:
Final Temp 1:
Hold Time:
Rate 2:
Final Temp 2:
Hold Time:
Run Time:
40¡C
1min
30¡C/min
190¡C
3min
10¡C/min
300¡C
5min
25.00min
Detector Parameters:
Detector Type
FID @ 310¡C
18
1.
2.
3.
4.
5
6.
7.
8.
9.
10.
11.
12.
13.
14.
15.
16.
17.
18.
19.
20.
21.
22.
19
2, 4, 5, 6 Ð tetrachloro Ð meta Ð xylene
α Ð BHC
γ Ð BHC
β- BHC
Heptachlor
δ - BHC
Aldrin
Heptachlorepoxy
gamma Ð chlordane
alpha Ð chlordane
Endosulfan A
p, pÕ Ð DDE
Dieldrin
Endrin
p, pÕ Ð DDD
Endosulfan B
p, p' - DDT
Endrin Aldehyde
Endosulfan Sulfate
Methoxychlor
Endrin Ketone
Decachlorobiphenyl
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