ANALYTICAL SOLUTIONS GCANALYTICAL SOLUTIONS

ANALYTICAL SOLUTIONS GCANALYTICAL SOLUTIONS

GC
ANALYTICAL
SOLUTIONS
ENV 82
ENVIRONMENTAL
Analysis of the US EPA8270 mix
on SolGel-1ms
SolGel-1ms, 0.25µ
µm film
10ppm in methanol
30m x 0.25 mm ID
40°C, 3 min.
8°C/min to 300°C,
300°C, 9 min.
Mass Spectrometer
He,
16 psi for 30 sec then drops to 10psi
10psi to 28psi at 0.5 psi/min
28psi until end of run.
1.1 mL/min.
On
Splitless
0.5 min
40mL/min
1 µL
250°C
No
4 mm ID Single Gooseneck
092017
054795
Full scan 41-450
Phase:
Sample:
Column:
Initial Temp:
Rate 1:
Final Temp:
Detector Type:
Carrier Gas:
Inlet Pressure
Pressure rate1:
Final Pressure:
Carrier Gas Flow:
Constant Flow:
Injection Mode:
Purge on Time:
Purge on (Split)Vent Flow:
Injection Volume:
Injection Temperature:
Autosampler:
Liner Type:
Liner Part Number:
Column Part Number:
Full Scan / SIM:
73, 74, 75
6000000
55
67, 68
5000000
29
16, 17
4, 5, 6
7,8 15
4000000
12
3000000
13
19
18
11
9
10
20
26
22
24
2123
37
33 38
36
30
31 34
25
32 35
28
2000000
14
2
44
41
3
52
50
47
40
1
58
62
63
66
64
56 59
39
46
43
49
76
70
69
71
42
53
57
48
45
1000000
65
51
72
60
78
77 79
61
82
54
81
83
27
0
5.00
10.00
15.00
20.00
25.00
30.00
35.00
40.00
Expanded view from 9.50-12.00 minutes
4, 5, 6
16,17
7,8
15
11
9
12
20
18
13
10
9.50
19
14
10.00
10.50
11.00
11.50
Expanded view from 12.40-14.20 minutes
12.00
29
26
21
23
22
24
30
31
25
28
27
12.40
12.60
12.80
13.00
13.20
13.40
13.60
13.80
14.00
14.20
Ti
Expanded view from 15.50-20.00 minutes
44
41
33
32
37
34
38
47
36
40
35
42
43
45
39
46
49
48
15.50
16.00
16.50
17.00
17.50
18.00
18.50
19.00
19.50
Components
1. Pyridine
2. n-Nitrosodimethylamine
3. 2-Fluorophenol
4. Phenol-d5
5. Phenol
6. Aniline
7. bis-(2-chloroethyl) ether
8. 2-Chlorophenol
9. 1,3-Dichlorobenzene
10. 1,4-Dichlorobenzene-d4
11. 1,4-Dichlorobenzene
12. 1,2-Dichlorobenzene
13. Benzyl alcohol
14. bis-(2-chloroisopropyl)ether
15. 2-Methyl phenol
16. n-Nitroso-di-n-propylamine
17. Hexachloroethane
18. 4-Methylphenol
19. Nitrobenzene-d5
20. Nitrobenzene
21. Isophorone
22. 2-Nitrophenol
23. 2,4-Xylenol
24. bis-(2-Chloroethoxy) methane
25. 2,4-Dichlorophenol
26. 1,2,4-Trichlorobenzene
27. Benzoic acid
28. Naphthalene-d8
29. Naphthalene
30. Hexachlorobutadiene
31. 4-Chloroaniline
32. 4-Chloro-3-methylphenol
33. 2-Methylnaphthalene
34. Hexachlorocyclopentadiene
35. 2,4,6-Trichlorophenol
36. 2,4,5-Trichlorophenol
37. 2-Fluorobiphenyl
38. 2-Chloronaphthalene
39. 2-Nitroaniline
40. Dimethyl phthalate
41. Acenaphthylene
42. 2,6-Dinitrotoluene
43. Acenaphthene-d10
44. Acenaphthene
45. 3-Nitroaniline
46. 2,4-Dinitrophenol
47. Dibenzofuran
48. 4-Nitrophenol
49. 2,4-Dinitrotoluene
50. Diethylphthalate
51. Fluorene
52. 4-Chlorophenyl phenyl ether
53. 2-Methyl-4,6-dinitrophenol
54. 4-Nitroaniline
55. n-Nitrosodiphenylamine
56. Azobenzene
57. 2,4,6-Tribromophenol
58. 4-Bromophenyl phenyl ether
59. Hexachlorobenzene
60. Pentachlorophenol
61. Phenanthrene-d10
62. Phenanthrene
63. Anthracene
64. Carbazole
65. Di-n-butyl phthalate
66. Fluoranthene
67. Benzidine
68. Pyrene
69. p-Terphenyl-d14
70. Butyl benzyl phthalate
71. Benz[a]anthracene
72. Chrysene-d12
73. 3,3-Dichlorobenzidine
74. Chrysene
75. bis(2-Ethylhexyl)phthalate
76. Di-n-octyl phthalate
77. Benzo[b]fluoranthene
78. Benzo[k]fluoranthene
79. Benzo[a]pyrene
80. Perylene-d12
81. Indeno[1,2,3-cd]perylene
82. Dibenz[a,h]anthracene
83. Benzo[g,h,i]perylene
SGE would like to thank Mark Ferry from ECS/MDL, USA for supplying the chromatograms and data for
this application
visit www.sge.com or contact our technical Customer Support Team on: [email protected]
SGE International Pty. Ltd.
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SGE, Incorporated (USA)
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SGE Europe Ltd. (UK)
email: [email protected]
SGE (France) Sarl
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SGE Deutschland GmbH
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SGE Japan Inc.
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SGE India
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