ANAL YTICAL SOLUTIONS GCANAL YTICAL SOLUTIONS

GC
ANAL YTICAL
SOLUTIONS
Analysis of US EPA 8081Organochlorine
ENV 72
ENVIRONMENTAL
Pesticide Mix on SolGel-1msTM
SolGel-1, 0.25µ
µm film
100ppm in Dichloromethane
30m x 0.25 mm ID
110°C, 1 min.
25°C/min to 150°C,
12°C/min to 260°C
15°C/min to 300°C
300°C, 5 min.
Mass Spectrometer
He, 31.6 psi
1.7 mL/min.
On
35 cm/sec at 110°C
Splitless
0.5 min.
60
1 µL
250°C
No
4 mm ID Single Taper Liner
092017
054795
113400
113409
Full scan 40-500
Phase:
Sample:
Column:
Initial Temp:
Rate 1:
Rate 2:
Rate 3:
Final Temp:
Detector Type:
Carrier Gas:
Carrier Gas Flow:
Constant Flow:
Average Linear Velocity:
Injection Mode:
Purge on Time:
Purge on (Split) Vent Flow:
Injection Volume:
Injection Temperature:
Autosampler:
Liner Type:
Liner Part Number:
Column Part Number:
ms-NoVent™ Part no.:
HP5973 restrictor:
Full Scan / SIM:
Components
1. 2,4,5,6-Tetrachloro-meta-xylene
2. α-BHC
3. β-BHC
4. γ-BHC
5. δ-BHC
6. Heptachlor
7. Aldrin
8. Heptachlorepoxy
9. trans-Chlordane
10. Endosulfan A
11. cis-Chlordane
12. pp-DDE
13. Dieldrin
14. Endrin
15. Endosulfan B
16. pp-DDD
17. Endrin aldehyde
18. Endosulfan sulfate
19. pp-DDT
20. Endrin Ketone
21. Methoxychlor
22. Decachlorobiphenyl
12
700000 0
9 11
6
600000 0
7
500000 0
2
400000 0
1
3
4
14
8
5
10
13
15
16
18
19
17
21
20
22
300000 0
200000 0
100000 0
0
6 .0 0
7 .0 0
8 .0 0
9 .0 0
1 0 .0 0
1 1 .0 0
1 2 .0 0
1 3 .0 0
1 4 .0 0
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